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UltraCLAVE

The UltraCLAVE can be used for semi-automated batch processing of samples and high-throughput or large-volume application and uses the patented SRC technology from Milestone. Loading, unloading and processing of samples is performed automatically under computer control. The UltraCLAVE allows processing of multiple samples—rotors with as many as 77 positions are available—or a single large reaction mixture. Reactions can be scaled from microliters to 3 litres, under identical conditions using the same reaction system. Continuous, unpulsed delivery of microwave power provides the most precise possible control over reaction conditions, from millisecond to millisecond

Features

• Largest volume single microwave reactor commercially available with 4,2 litre reaction chamber

• High pressure and temperature reactor up to 200 bar and 260°C in 3.5 litre PTFE internal vessel

• High throughput.process with up to 40 samples per batch without the need for capping or uncapping.

• All parts in contact with reagents in high resistant steel and ceramic or PTFE liners and coating.

• Identical temperature and pressure conditions for all samples. with no cross-contamination

• Automatic opening/closing of the pressure vessel with built in exhaust of solvent and acid vapours

• Disposable vessel option with direct to ICP for analysis

• Advanced integrated terminal with user friendly EasyCLAVE Software, full GLP documentation

The high pressure steel reactor has a volume of 4.2 litres and an effective working volume of 3.5 litres with the PTFE liner installed. Microwave energy from the system's magnetron is introduced into the reactor through a special microwave-transparent port. Since the reactor and cavity are the same, the internal geometry is optimised for direct microwave coupling to materials in the reactor, this design ensures maximum sample heating efficiency. The interior of the UltraCLAVE stainless steel reactor is protected by a special surface treatment for acid and chemical resistance.

The EasyCLAVE software includes an Autorun mode in which a complete procedure is automatically run. The user is only required to set the Start and Stop parameters, place the sample container/rack in the UltraCLAVE and press Autorun. The unit will automatically close, reach the preset load pressure, carry out the temperature/pressure program, stop the program and release pressure. After pressure release the system will automatically open. An email can be sent to a specific email address advising the procedure is completed. Full documentation is available as well as a solvent library for increased safety of operation.

High temperature, high pressure, high throughput system